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投稿时间：2025-03-20
投稿时间：2025-03-20
中文摘要: 为优化化橘红挥发油的提取工艺，并对其化学成分进行分析，该试验采用水蒸气蒸馏法，结合单因素试验考察浸泡时间、提取时间以及固液比对化橘红挥发油提取率的影响，设计三因素三水平的正交试验，优化得出最佳的提取工艺，同时运用气相色谱-质谱联用（gas chromatography-mass spectrometry，GC-MS）技术对化橘红挥发油成分进行分析。结果表明，最佳提取工艺条件为浸泡时间2 h、提取时间5 h、固液比1∶8 （g/mL）；按照最佳提取工艺进行3 次验证，得到化橘红挥发油的平均提取率为0.42%，应用GC-MS对化橘红挥发油含有的化学成分进行分析，通过谱库共鉴定出挥发油中含有43 个化学成分，得出4 种化学成分含量较高，分别为β-月桂烯、邻伞花烃、柠檬烯、γ-松油烯，含量之和为81.56%。
中文关键词: 化橘红 挥发油 提取工艺 气相色谱-质谱法（GC-MS） 化学成分
Abstract:To optimize the extraction process of volatile oil from Exocarpium Citri Grandis，and its chemical components were analyzed. The steam distillation method was adopted. Single-factor experiments were conducted to investigate the effects of soaking time，extraction time，and solid-liquid ratio on the extraction rate of volatile oil. An orthogonal test with three factors and three levels was designed to optimize the extraction process. Meanwhile，gas chromatography-mass spectrometry （GC-MS） was used to analyze the components of the volatile oil. The results showed that the optimal extraction conditions were as follows：soaking time of 2 h，extraction time of 5 h，and solid-liquid ratio of 1∶8 （g/mL）. Three verification tests were performed under the optimal conditions，and the average extraction rate of volatile oil was 0.42%. A total of 43 chemical components were identified from the volatile oil by GC-MS library search. Four components with high content were found，including β-myrcene，o-cymene，limonene，and γ-terpinene，with a total content of 81.56%.
keywords: Exocarpium Citri Grandis volatile oil extraction process gas chromatography-mass spectrometry（GC-MS） chemical component
文章编号：202612019 中图分类号： 文献标志码：
基金项目:福建中烟科技重点项目（FJZYKJJH2024ZD008）
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