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食品研究与开发:2023,44(7):157-162
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婴幼儿配方食品中矿物元素的检测
(1.四川省食品检验研究院,四川 成都 610097;2.国家市场监管重点实验室(白酒监管技术),四川 成都 610097;3.成都医学院,四川 成都 611137)
Detection of Mineral Elements in Infant Formula Food
(1.Sichuan Institute of Food Inspection,Chengdu 610097,Sichuan,China;2.Key Laboratory of Baijiu Supervising Technology for State Market Regulation,Chengdu 610097,Sichuan,China;3.Chengdu Medical College,Chengdu 611137,Sichuan,China)
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投稿时间:2022-02-15    
中文摘要: 为解决部分婴幼儿配方食品中矿物元素检测不均的问题,采用干法、湿法、微波法和复溶-微波法对样品进行消解检测,结果表明:干法消解的数据质量最差;湿法与微波消解法检测的结果相比,铜、铁、钾、镁、锰和钠的含量差异不显著(P>0.05),部分矿物元素(铜、铁、钾、钠、磷、锌)检测结果的相对标准偏差(relative standard deviation,RSD)减小,但未达到预期。样品复溶后进行微波消解检测发现,用水复溶后的大部分元素含量偏低,特别是铁,且检测的矿物元素RSD 均较大,而用5%硝酸复溶后,元素含量均没有明显偏高和偏低,且RSD 均明显减小。因此,通过5%硝酸复溶样品后进行微波消解检测婴幼儿配方食品中的矿物元素,可以解决样品中矿物元素测定结果不均的问题。
Abstract:To solve the uneven detection of mineral elements in some infant formula food,this study used the dry method,wet method,microwave method,and reconstitution-microwave method to digest and detect samples.The results showed that the data quality of the dry method was the worst. As compared with the microwave method,the content of copper,iron,potassium,magnesium,manganese,and sodium of the wet method had no significant difference(P>0.05),and the relative standard deviation(RSD)of the detection results of some mineral elements(copper,iron,potassium,sodium,phosphorus,and zinc)was decreased but did not meet the expectations. The detection by the microwave method showed that after the samples were reconstituted,the content of most elements was low when samples were reconstituted with water,especially that of iron,and the RSD was relatively large. However,when samples were reconstituted with 5% nitric acid,the content was not significantly higher or lower,but the RSD was significantly reduced. Therefore,the detection of mineral elements in infant formula food by the microwave method after the reconstitution of samples with 5% nitric acid can solve the problem of uneven detection of mineral elements in samples.
文章编号:202307022     中图分类号:    文献标志码:
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