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投稿时间：2018-08-30
投稿时间：2018-08-30
中文摘要: 建立以超高效液相色谱-串联三重四级杆质谱同时测定辣椒酱中18种非食用色素的有效方法。样品通过MgSO4 和 NaCl 协同乙腈振荡提取，提取液经 QuEChERS（quick、easy、cheap、effective、rugged、safe 的简称）填料净化后采用多反应监测（multiple reaction monitoring，MRM）模式进行测定。结果表明：18种非食用色素的定量限为6.0 μg/kg～51.0 μg/kg，回收率为80.2%～109.2%，相对标准偏差为2.4%～9.7%。该方法实现了多种非食用色素的同时分析，适用于打击辣椒酱中非法添加非食用色素的快速检测。
中文关键词: 超高效液相色谱-串联三重四级杆质谱 辣椒酱 非食用色素 QuEChERS 快速测定
Abstract:Methods to determine 18 non-edible pigments in chili sauce had been established by ultra performance liquid chromatography-mass spectrometry mass spectrometry（UPLC-MS/MS）.Samples were extracted by MgSO4 and NaCl accompanied with acetonitrile first，and then purified by QuEChERS（quick，easy，cheap，effective，rugged，safe） paddings.The target compounds were detected by multiple reaction monitoring（MRM）mode finally.The experimental results showed that the quantitation limits of the 18 nonedible pigments vary from 6.0 μg/kg-51.0 μg/kg，the average recoveries ranging from 80.2%to 109.2%，the relative standard deviations 2.4 % to 9.7 %.This method is simple，rapid and efficient，and it can meet the requirement of simultaneous determination of non-edible pigments in chili sauce，contributing to attack illegal addition of non-edible pigments in chili sauce.
keywords: ultra performance liquid chromatography-mass spectrometry mass spectrometry（UPLC-MSMS） chili sauce non-edible pigments QuEChERS rapid determination
文章编号：201911031 中图分类号： 文献标志码：
基金项目:南昌市指导性科技计划项目（洪科发计字[2016]96号第83 项）
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