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食品研究与开发:2018,39(6):46-52
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响应面法优化山药抗性淀粉制备及结构分析
张红霞1,2,金佳幸1,2,李炎1,张玉涛1,2,龙菊1
(1.安顺学院化学化工学院,贵州安顺561000;2.贵州省教育厅功能材料与资源化学特色重点实验室,贵州安顺561000)
Optimization of Preparation for Chinese Yam by Response Surface Methodology and Structural Analysis
ZHANG Hong-xia1,2,JIN Jia-xing1,2,LI Yan1,ZHANG Yu-tao1,2,LONG Ju1
(1.School of Chemistry and Chemical Engineering,Anshun University,Anshun 561000,Guizhou,China;2.Special and Key Laboratory of Functional Materials and Resource Chemistry of Guizhou Provincial Education Department,Anshun 561000,Guizhou,China)
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投稿时间:2017-10-13    
中文摘要: 以安顺山药为原料,通过单因素试验(one-factor-at-a-time method,OFAT)及响应面分析法(response surface methodology,RSM)优化压热法制备抗性淀粉(resistant starch,RS)的工艺,并对抗性淀粉的结构进行X-射线衍射仪(X-Ray Diffraction,XRD)、傅立叶红外光谱仪(Fourier Transform Infrared Spectrometer,FT-IR)和扫描电镜(Scanning Electron Microscope,SEM)等表征分析。结果显示:通过工艺条件优化,在淀粉乳百分含量为14%,pH值为6.0,压热温度为112℃,压热时间为1.5 h时,抗性淀粉得率为24.83%,与响应面预测值高度相符,结果合理可靠。
中文关键词: 安顺山药  抗性淀粉  压热法  响应面法
Abstract:Using Anshun yam as the experimental material,one-factor-at-a-time method and response surface methodology were applied to optimize the autoclave method for preparing resistant starch.Meanwhile,the structure of yam RS was analyzed by X-Ray Diffraction,Fourier Transform Infrared Spectrometer and Scanning Electron Microscope.It was found that by optimizing the preparation process,the yield of resistant starch was 24.83%when the starch milk percentage was 14%,pH value was 6.0,pressure heat temperature was 112℃and pressure heat time was 1.5 h respectively.The experimental value was highly agreed with the predicted value of response surface.
文章编号:201806009     中图分类号:    文献标志码:
基金项目:国家自然科学基金(41403114);贵州省科技合作计划项目(黔科合J字LKA[2013]06号、黔科合J字LKA[2012]05号);贵州省教育厅自然科学研究项目(黔教科合KY字[2013]178号);贵州省大学生创新创业训练计划项目(201610667008)
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