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投稿时间：2016-05-18
投稿时间：2016-05-18
中文摘要: 建立高效液相色谱法测定葡萄酒中白藜芦醇的方法，考察直接进样法的检测波长、洗脱强度、流动相 pH 值、柱 温、样品 pH 值等因素对酒样分离的影响，建立 HPLC 检测葡萄酒中白藜芦醇的方法，相关系数 r 为 0.999 9 ，线性范 围为 1 mg/L ~20 mg/L，精密度、稳定性、回收率试验的 RSD 分别为 1.16 %、2.9 %和 1.25 %，酒样检测发现白藜芦醇的含 量随酒的年份和品种变化，品种间比较结果为：蛇龙珠最优，梅鹿辄、赤霞珠、霞多丽次之，贵人香最低，其中蛇龙珠含量 高达 6 mg/L。
Abstract:The effects of detection wavelength，solvent strength，mobile phase pH，column temperature， sample pH and other factors on the separation of wines were examined.A direct injection HPLC method for determina－ tion of resveratrol in wine was established. The correlation coefficient r was 0.999 9， linear range was 1 mg /L-20 mg/L， RSD of precision experiment， stability experiment and recovery experiment were 1.16 %， 2.9 % and 1.25 % respectively.It was found that resveratrol content of wines varied with years and varieties，its changing law was：Cabernet Gernischt was the best chioce，Merlot and Cabernet Sauvignon and Chardonnay took second， the last was Riesling. Resveratrol content in Cabernet Gernischt was up to 6 mg /L.
keywords: resveratrol HPLC rate of recovery wine
文章编号：201705033 中图分类号： 文献标志码：A
基金项目:国家自然科学基金项目（31401480）
| Author Name | Affiliation |
| FENG Yu-qin， GUO Hong-yan， LIU Gui-shan*， HE Jian-guo，WANG Song-lei， HE Xiao-guang | Agricultural College ，Ningxia University， Yinchuan 750021， Ningxia， China |
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