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投稿时间:2022-04-18
投稿时间:2022-04-18
中文摘要: 以菜籽油、亚麻籽油、青藏高原牦牛酥油为原料,分别按照牦牛酥油∶亚麻籽油∶菜籽油质量比为1∶2∶7(A)、1∶1∶8(B)、2∶1∶7(C)制备调和油,通过单因素试验和正交试验分别确定3种调和油中牦牛酥油溶解率的最佳工艺条件;利用气相色谱-质谱法(gas chromatography-mass spectrometry,GC-MS)分别对3种调和油及其沉淀进行脂肪酸组成分析。结果表明,3种调和油均无异味,酸值、过氧化值均符合国家食用油标准,油脂品质高、稳定性强、不易变质;所有调和油及其沉淀物质共检出脂肪酸44种,单一样品脂肪酸检出种类在39种~44种之间;共检出8种支链脂肪酸,其中,调和油C中支链脂肪酸含量最多,为2.92%;3种调和油中检出的主要脂肪酸为棕榈酸、亚麻酸、亚油酸、油酸,ω-6、ω-3脂肪酸含量的比值在1.29~1.80之间,从营养价值角度出发,调和油A中ω-6脂肪酸和ω-3脂肪酸比值较小,脂肪酸含量的比例更接近1∶1。
Abstract:Rapeseed oil,flaxseed oil and yak ghee were used to prepare the blend oils according to the mass ratios of yak ghee ∶flaxseed oil∶rapeseed oil at 1 ∶2 ∶7(A),1 ∶1 ∶8(B)and 2 ∶1 ∶7(C),respectively.The optimal conditions for the solubility of yak ghee in the three blend oils were determined by single factor test and orthogonal test.The fatty acid composition of the three blend oils and their precipitates was analyzed by gas chromatography-mass spectrometry(GC-MS).The results showed that the three blend oils had no peculiar smell,with the acid value and peroxide value meeting the national standards of edible oils,demonstrating high quality and strong stability and 44 of fatty acids were detected in all the blend oils and their precipitates.The number of fatty acids detected in single samples ranged from 39 to 44.A total of 8 branched chain fatty acids were detected,which had the highest content(2.92%)in the blend oil C.The main fatty acids in the three oils included palmitic acid,linolenic acid,linoleic acid,and oleic acid.The ω-6/ω-3 ratios varied within the range of 1.29-1.80,From the perspective of nutritional value,the ratio of ω-6 fatty acids to ω-3 fatty acids in mixed oil A was closer to 1∶1.
keywords: yak ghee linseed oil rapeseed oil blend oil gas chromatography-mass spectrometry(GC-MS) fatty acid
文章编号:202217003 中图分类号: 文献标志码:
基金项目:国家自然科学基金项目(22167020)
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