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食品研究与开发:2022,43(12):164-176
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HS-SPME-GC-MS法分析3种加工工艺牛蒡茶特征性风味物质
(1.徐州工程学院食品与生物工程学院,江苏 徐州 221018;2.徐州生物工程职业技术学院,江苏 徐州 221006)
Identification of Characteristic Flavor Compounds in Burdock Tea Processed with Three Methods by HS-SPME-GC-MS
(1.School of Food and Biology Engineering,Xuzhou University of Technology,Xuzhou 221018,Jiangsu,China;2.Xuzhou Vocational College of Bioengineering,Xuzhou 221006,Jiangsu,China)
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投稿时间:2021-08-03    
中文摘要: 为研究3种不同加工工艺牛蒡茶中特征性风味物质,采用顶空-固相微萃取(headspace-solid phase microextraction,HS-SPME)和气相色谱-质谱(gas chromatography-mass spectrometry,GC-MS)联用法测定其组成,经主成分分析(principal component analysis,PCA)和活性值比较,筛选确定牛蒡茶共有的特征性风味物质,探讨3种加工工艺牛蒡茶的主体风味物质。结果表明:3种加工工艺牛蒡茶共检测出97种挥发性成分,其中酮类12种,醛类19种,酯类12种,醇类7种,烷烃类15种,酸类7种,吡嗪类9种,其他(呋喃、烯)类17种,以醛类化合物为主。经主成分分析,贡献较大的风味物质有64种,其中2-乙基-6-甲基-吡嗪、2-乙酰基吡啶、戊醛、2-丁基-2-辛烯醇等10种成分具有较高活性值,是牛蒡茶的特征性风味物质,赋予其烘烤、苹果、杏仁且略带泥土清香的风味。2,5-二甲基吡嗪、1-(2-呋喃基)-乙酮和异戊醛分别是3种加工工艺牛蒡茶的主体风味物质。
Abstract:To identify the characteristic flavor compounds in the burdock tea processed with three different methods,headspace-solid phase microextraction (HS-SPME)and gas chromatography-mass spectrometry(GC-MS)were employed to determine the chemical composition of the tea samples.Principal component analysis(PCA)and odor activity value comparison were conducted to identify the common and specific flavor compounds in the burdock tea processed with three different methods.A total of 97 volatile components were detected in burdock tea,including 12 ketones,19 aldehydes,12 esters,7 alcohols,15 alkanes,7 acids,9 pyazines,and 17 other(furan,alkene)compounds.PCA identified 64 flavor compounds with great contributions,among which 10 with high odor activity values,such as 2-ethyl-6-methyl-pyrazine,2-acetyl-pyridine,valeraldehyde,and 2-butyl-2-octenol,were the characteristic flavor substances of burdock tea.These characteristic flavor compounds endow burdock tea with baked,apple,almond,and slightly earthen flavor.Specifically,2,5-dimethylpyrazine,1-(2-furanyl)-acetone,and isovaleraldehyde were the specific flavor compounds of burdock tea processed with three different methods,respectively.
文章编号:202212022     中图分类号:    文献标志码:
基金项目:国家自然科学基金项目(31401553);江苏省科技计划项目(苏北科技专项)(XZ-SZ201803);江苏高校“青蓝工程”资助项目(苏教师(2018)12号)
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