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食品研究与开发:2021,42(16):99-106
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红毛藻复合脱腥工艺的优化及其挥发性成分GC-MS分析
(1.集美大学食品与生物工程学院,福建 厦门 361021;2.福建省食品微生物与酶工程重点实验室,福建 厦门 361021;3.厦门市食品生物工程技术研究中心,福建 厦门 361021)
Optimization of Compound Deodorization Progress and GC-MS Analysis of Volatile Components of Bangia fusco-purpurea
(1.College of Food and Biology Engineering,Jimei University,Xiamen 361021,Fujian,China;2.Fujian Provincial Key Laboratory of Food Microbiology and Enzyme Engineering,Xiamen 361021,Fujian,China;3.Research Center of Food Biotechnology of Xiamen City,Xiamen 361021,Fujian,China)
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投稿时间:2020-03-18    
中文摘要: 红毛藻是特色药食两用红藻资源,腥味是限制红毛藻深加工产品开发的关键因素之一。该文对红毛藻复合脱腥加热联用浸泡脱腥剂工艺进行优化,并应用气相色谱-质谱联用(gas chromatography-mass spectrometry,GC-MS)分析脱腥前后挥发性成分。结果表明,复合脱腥可显著降低红毛藻的腥味,最优脱腥工艺为加热温度70℃,加热时间4 h,醋酸浓度3%,醋酸处理时间2.0 h。脱腥前红毛藻含有醇类、烯烃、醛类、酮类、酯类、烷烃类和其它类共7大类46种挥发性成分,其中1-辛烯-3-醇、壬醛、2-壬烯醛、2,4-癸二烯醛和3,5-辛二烯-2-酮为腥味成分;复合脱腥后,挥发性成分由46种变为26种,醇类、醛类和酮类物质明显减少,烷烃类和其它类物质明显增多,上述腥味成分含量除壬醛由44.40μg/g降为37.89μg/g外,其它均降为0。
Abstract:Bangia fusco-purpurea is a special medicinal and edible red algae resource.The development of advanced processing products of B.fusco-purpurea has been hindered by the fishy odor.In this paper,B.fuscopurpurea compound deodorization combining heating with soaking in deodorant for was optimized.Gas chromatography-mass spectrometry(GC-MS)was used to analyze the volatile components of B.fusco-purpurea before and after compound deodorization.Compound deodorization significantly reduced the fishy odor of B.fusco-purpurea.The optimal deodorization conditions were a heating temperature of 70 ℃,heating time of 4 h,acetic acid concentration of 3%,and acetic acid treatment time of 2.0 h.GC-MS of undeodorized B.fuscopurpurea revealed 46 volatiles in seven categories,including alcohols,aldehydes,ketones,alkanes,olefins,esters and others.1-octen-3-ol,nonanal,2-nonenal,2,4-decadienal,and 3,5-octadien-2-one contributed to the fishy odor.After compound deodorization,26 volatile components were present.Alcohols,aldehydes,and ketones were significantly reduced,while alkanes and other components were obviously increased.Nonanal was reduced from 44.40 μg/g to 37.89 μg/g,the contents of other fishy odor components were undetectable.
文章编号:202116015     中图分类号:    文献标志码:
基金项目:福建省科技厅重点项目(2018N0019);福建省自然科学基金资助项目(2019J01697)
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