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食品研究与开发:2020,41(16):120-125
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响应曲面优化离子液体-微波辅助提取黑豆皮中花青素的工艺研究
(绥化学院食品与制药工程学院,黑龙江绥化152061)
Response Surface Methodology for Optimizing the Extraction of Anthocyanins from Black Soybean Peel by Ionic Liquids-Microwave-assisted Extraction
(Food and Pharmaceutical Engineering Department,Suihua University,Suihua 152061,Heilongjiang,China)
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投稿时间:2019-08-28    
中文摘要: 为高效获得花青素,采用离子液体-微波辅助提取黑豆皮中的花青素,考察提取时间、提取温度、微波功率、离子液体浓度、料液比对提取量的影响,采用响应曲面法对提取工艺进行优化。结果表明,最佳提取条件为提取时间45 min,离子液体浓度0.7 mol/L,料液比1∶30(g/mL),微波功率460 W,提取温度49℃。在此条件下,花青素的提取量为4.834 mg/g,预测值和实际测定值接近,可以为黑豆皮花青素后续的利用和研发提供参考。
Abstract:In order to obtain anthocyanin efficiently,the extraction of black soybean coats anthocyanin by ionic liquid ultrasound was studied.The effects of extraction time,temperature,microwave power,ionic liquid concentration and solid-liquid ratio on the extraction amount were investigated.The extraction process was optimized by response surface methodology.The results showed that the optimum extraction conditions were as follows:extraction time 45 min,ionic liquid concentration 0.7 mol/L,solid-liquid ratio 1 ∶30(g/mL),microwave power 460 W,extraction temperature 49℃.Under these conditions,the yield of anthocyanin from black soybean coats was 4.834 mg/g,and the predicted value is close to the actual measured value,which can provide a basis for the comprehensive development and follow-up research of anthocyanin from black soybean coats.
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