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食品研究与开发:2019,40(20):137-142
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苦荞麦米黄酮提取的两种工艺研究
(河北师范大学化学与材料科学学院,河北石家庄050024)
Study on Two Extraction Processes of Flavonoids in Tartary Buckwheat
(College of Chemistry and Material Sciences,Hebei Normal University,Shijiazhuang 050024,Hebei,China)
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投稿时间:2018-11-28    
中文摘要: 通过考察乙醇浓度、温度、料液比、提取时间4 个因素对总黄酮提取率的影响获得提取苦荞麦米黄酮的最佳工艺。利用单因素试验和正交试验确定超声波法辅助提取苦荞麦米中总黄酮的最佳工艺为:乙醇浓度70 %,料液比1 ∶70(g/mL),温度为80 ℃,提取时间为50 min。在此条件下,苦荞麦米中总黄酮的提取率为4.128%;恒温水浴法提取苦荞麦米中总黄酮的最佳工艺为:乙醇浓度80%,料液比1 ∶70(g/mL),温度为70 ℃,提取时间为80 min。在此条件下,苦荞麦米中总黄酮的提取率为4.477%。通过比较发现,两种方法提取的黄酮含量相差不大,超声法辅助提取的时间相对较短,节能。因此,超声法辅助提取苦荞麦米中的黄酮比恒温水浴法的效果好。
中文关键词: 苦荞麦米  超声波法  恒温水浴法  黄酮  醇提
Abstract:The best technological way of extract flavonoids was determined by examining the impact of ethanol concentration,temperature,ratio of material to liquid and extraction time on extraction rate of flavonoids.By using single factor test and orthogonal test,this research indentified that the optimal process conditions of ultrasonic method to extract flavonoids in tartary buckwheat were as follows:ethanol concentration was 70 %,ratio of material to liquid was 1 ∶70(g/mL),temperature was 80 ℃ and extraction time was 50 min.Under such process conditions,extraction rate of flavonoids was 4.128 %.The optimal process conditions of constant temperature water bath method to extract flavonoids in tartary buckwheat were as follows:ethanol concentration was 80%,ratio of material to liquid was 1 ∶70(g/mL),temperature was 70 ℃ and extraction time was 80 min.Under such process conditions,extraction rate of flavonoids was 4.477%.By comparing the two methods,it was found that the content of flavonoids extracted by the two methods had little difference,the extraction time by ultrasonic method was relatively short,energy saving were found.Therefore,the effect of ultrasonic-assisted extraction of flavonoids from tartary buckwheat wheat rice was better than that of constant temperature water bath method.
文章编号:201920025     中图分类号:    文献标志码:
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