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食品研究与开发:2019,40(19):59-64
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低吸湿性高分子复合胶囊的制备及性能研究
LI Lu,BAO Sui,ZHANG Li-ming,WANG Ran,YANG Xing-xiang,TANG Shu-jun
(1.China Tobacco Anhui Industrial Co.,Ltd.,Hefei 230031,Anhui,China;2.CASHefeiInstitute of Technology Innovation Co.,Ltd.,Hefei 230088,Anhui,China)
Preparation and Properties of Low Hygroscopic Polymer Composite Capsules
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投稿时间:2019-03-18    
中文摘要: 通过不同比例卡拉胶/魔芋胶共混和低交联的方法制备一种低吸湿性的高分子复合胶囊剂。利用黏度仪、扫描电子显微镜和胶囊破碎强度测试仪等分析手段对材料进行表征。结果表明:直接共混的复合胶囊剂无色无味、透明度高,在相同温度和转速下测试可知,随着魔芋胶含量的增加,溶液黏度先增大后降低,其卡拉胶/魔芋胶最优质量比为3 ∶1,此时体系黏度为589 mPa·s,用滴丸机制成胶囊,其破碎强度可达到15.4 N;加入交联剂后,体系黏度逐渐增大,交联剂的比例加入至2.5%时,体系黏度增加至890 mPa·s,胶囊成品的破碎强度可达到24 N。吸湿性能测试表明,材料的吸湿性受环境影响较大,湿度增大时,吸水平衡时的吸水量大。加入交联剂后的体系,材料吸水率明显下降。
Abstract:A low hygroscopic polymer composite capsule was prepared by different ratios of carrageenan/konjac blending and low cross-linking.The materials were characterized by viscometer,scanning electron microscope and capsule hardness tester.The results showed that the directly blended composite capsules were colorless,odorless and highly transparent.At the same temperature and speed,solution viscosity increased first and then decreased with the increase of konjac content.The optimal compounding mass ratio was 3 ∶1,and viscosity was 589 mPa·s,and the capsule was made by pill dropping machine,with a crushing strength of 15.4 N.After adding the crosslinking agent,the viscosity of the system gradually increased,and the crosslinking was achieved.When the proportion of the agent was added to 2.5 %,the viscosity of the system was increased to 890 mPa·s,with a crushing strength of 24 N.The moisture absorption performance test showed that the hygroscopicity of the material was greatly affected by the environment,and when the humidity was increased,the water absorption amount at the time of water absorption balance was larger.However,the water absorption rate of the material decreased significantly after the addition of the crosslinking agent.
文章编号:201919011     中图分类号:    文献标志码:
基金项目:安徽省科技重大专项(18030901083);中国科学院科技服务网络计划(KJF-STS-SCYD-203);安徽中烟集团科学项目(2017134)
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