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投稿时间：2018-05-17
投稿时间：2018-05-17
中文摘要: 采用高效液相色谱法测定衢枳壳中新橙皮苷及柚皮苷含量。色谱柱为Waters Symmetry C18（250 mm×4.6 mm，5 μm），流动相为乙腈-水（体积比为20∶80）；检测波长为283 nm；流速：1.0 mL/min。新橙皮苷和柚皮苷分别在0.191 μg/mL～3.056 μg/mL和0.195 μg/mL～3.120 μg/mL范围内呈良好的线性关系，其平均回收率分别为95.8%和96.1%，RSD分别为2.1%和2.0%。新橙皮苷和柚皮苷的平均回收率分别为95.8%和96.1%。
Abstract:A sensitive high performance liquid chromatography（HPLC）method was established for determine of neohesperidin and naringin in quzhiqiao.Neohesperidin and naringin were separated on a Waters Symmetry C18（250 mm×4.6 mm，5 μm）column with acetonitrile-water（volume ratio of 20 ∶80）as the mobile phase and detected at 283 nm.The flow rate was 1.0 mL/min.The calibration curves were linear in the ranges of 0.191 μg/mL-3.056 μg/mL and 0.195 μg/mL-3.120 μg/mL for neohesperidin and naringin respectively.The average recoveries were 95.8%and 96.1%the RSD were 2.1%and 2.0%.
keywords: quzhiqiao citrus changshan-huyou neohesperidin naringin high performance liquid chromatography（HPLC）
文章编号：201821027 中图分类号： 文献标志码：
基金项目:常山县科技计划项目（2017010）
| Author Name | Affiliation |
| YAN Xiao-li，YAN Qian-qian，LIU Xiao-zheng，HUANG Hao-xia，ZHENG Zhi-you，SHI Tang-hong | （Testing Center for Fruit Quality of Zhejiang Province，Changshan 324200，Zhejiang，China） |
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