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投稿时间:2017-02-26
投稿时间:2017-02-26
中文摘要: 采用单因素试验优化顶空固相微萃取(headspace-solid phase micro extraction,HS-SPME)条件,并结合气相色谱-质谱(gas chromatograph-mass spectrometer,GC-MS)联用技术,分析红树莓果醋自然发酵和纯种发酵的香气成分。结果表明:经GC-MS分析两种不同工艺红树莓果醋共鉴定出84种香气成分,32种是两者共有的,两种红树莓果醋的主要香气成分都为苯乙醇、苯甲酸乙酯、乙酸乙酯、α-紫罗兰酮和β-紫罗兰酮,自然发酵相对含量分别为26.12%、9.91%、8.51%、5.64%和4.09%,纯种发酵相对含量分别为22.39%、3.43%、32.68%、3.32%和2.81%。此外,根据感官评价,纯种发酵的果醋优于自然发酵,醋香浓郁,色泽饱满,口感绵延柔和,更具红树莓果醋典型性风味。
中文关键词: 固相微萃取 气相色谱-质谱联用技术 红树莓果醋 香气成分
Abstract:The aromatic compositions of red raspberry vinegar fermented with one step and two steps under two different fermentation processes were analyzed by headspace solid-phase micro-extraction(HS-SPME)coupled to gas chromatography-mass spectrometry (GC-MS).The results showed that a total of 84 kinds of aroma components were identified under the two different vinegar-making processes.32 kinds of aroma components were detected in vinegars fermented nature and pure breed.The main aroma components in two red raspberry vinegars were benzene ethanol,benzoic acid ethyl ester,ethyl acetate,α-ionone and β-ionone of which,the relative contents of nature fermented vinegar were 26.12%,9.91%,8.51%,5.64%and 4.09%respectively,and the relative contents of pure breed fermented vinegar were 22.39%,3.43%32.68%,3.32%and 2.81%respectively.According to the sensory evaluation,the vinegar fermented with pure breed fermentation was superior to that the vinegar fermented with nature fermentation.Nature fermented red raspberry vinegar was clear and transparent,the color was full,the taste was mellow and soft,the fragrance was lovely and lasting,and of more red raspberry vinegar typical flavor.
keywords: solid-phase micro-extraction(SPME) gas chromatography-mass spectrometry(GC-MS) red raspberry vinegar aromatic compositions
文章编号:201721023 中图分类号: 文献标志码:
基金项目:北京电子科技职业学院科研团队项目(TD201602);北京市教委科技计划面上项目(KM201510858001);促进高校内涵建设-教育教学类-大学生科研训练(CJGX2016-JX-07)
Author Name | Affiliation |
ZHANG Qiang,YU Xue-lian,CHEN Liang*,XIN Xiu-lan,CHANG Li,WEN Yi,ZHANG Hai-ting | College of Bioengineering,Beijing Polytechnic,Beijing 100029,China |
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