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食品研究与开发:2017,38(14):161-163
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气相色谱法同时测定食品中8种防腐剂
周家萍1,李典2,李治东2,崖薷丹2,降升平1,杨志岩1
(1.天津科技大学 现代分析技术研究中心,天津 300457;2.天津科技大学 食品工程与生物技术学院, 天津 300457)
Simultaneous Determination of 8 Preservatives in Foods by Gas Chromatography
ZHOU Jia-ping1, LI Dian2, LI Zhi-dong2,YA Ru-dan2, JIANG Sheng-ping1, YANG Zhi-yan1
(1. Research Center for Modern Analysis Techniques, Tianjin University of Science and Technology, TianJin 300457, China; 2. College of Food Engineering and Biotechnology, Tianjin University of Science and Technology, Tianjin 300457, China)
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本文已被:浏览 5628次   下载 3619
投稿时间:2016-03-18    
中文摘要: 针对食品中的添加剂,如何能够快速准确的进行定性定量分析,是衡量其安全性的前提条件。气相色谱法是 一种具有高分离能力的分析方法,该法具有分析时间短、分析成本低、样品前处理过程简单等特点。采用气相色谱 法作为检测防腐剂的基本方法,主要针对食品中丙酸、山梨酸、苯甲酸、脱氢乙酸、对羟基苯甲酸甲酯、对羟基苯甲 酸乙酯、对羟基苯甲酸丙酯、对羟基苯甲酸丁酯等 8 种防腐剂进行分析,结果显示,这些目标物都能够得到较好的 分离。通过对各类酱油、饮料中防腐剂的种类与含量进行分析,得到较好结果,为食品中酱油和饮料安全性评价提 供基础。
中文关键词: 酱油  饮料  气相色谱  防腐剂
Abstract:It is a prerequisite for the safety of additives in food to be able to carry out qualitative and quantitative analysis quickly and accurately. Gas chromatography is a kind of analytical method with high separation ability. The method has the characteristics of short analysis time, low analytical cost, simple sample pretreatment pro- cess. To establish a GC-FID method for the simultaneous determination of 8 preservatives in soybean sauce, vinegar, beverage. These include propanoic acid, sorbic acid, benzoic acid, Dehydroacetic, Methyl 4 -hy- droxybenzoate, Ethyl 4-hydroxybenzoate, Propylparaben, Butyl paraben. The results showed that these objects could be better separated. Through the analysis of the types and contents of preservatives in various kinds of soy sauce and beverage, the results were obtained, which provided the basis for the safety evaluation of soy sauce and beverage in food.
文章编号:201714034     中图分类号:    文献标志码:A
基金项目:天津科技大学实验室开放基金(1431A305)
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