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食品研究与开发:2016,37(12):-
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响应面法优化绞股蓝皂苷微波辅助-超声提取工艺
(1.闽南师范大学化学与环境学院,福建漳州363000;2.福建省现代分离分析科学与技术重点实验室,福建漳州363000)
Optimization of Microwave-ultrasonic-assisted Extraction of Saponins from Gynostemmapentaphyllum Using Response Surface Methodology
(1.Colllege of Chemistry and Environment,Minnan Normal University,Zhangzhou 363000,Fujian,China;2.Fujian Province Key Laboratory of Morden Analytical Science and Separation Technology,Zhangzhou 363000,Fujian,China)
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投稿时间:2015-01-19    
中文摘要: 以绞股蓝为原料,采用微波超声双辅助提取皂苷。在单因素试验的基础上,采用响应面分析法优化提取工艺,建立二次多项数学模型。结果表明,绞股蓝皂苷微波超声双辅助提取的最优工艺参数为:微波功率400 W、超声时间60 min、乙醇浓度80%、超声温度为51℃、微波时间117 s、液料比28∶1(mL/g),此条件下绞股蓝皂苷提取率为7.05%,与预测值的相对误差约为0.57%,试验值与预测值相吻合。
Abstract:The microwave-ultrasonic-assisted extraction ofsaponins from Gynostemma pentaphyllum was optimized using response surface methodology.Base on single-factor experiments,the extraction conditions ofmicrowave-ultrasonic-assisted extraction yield of saponins in the Gynostemma pentaphyllum were by RSM.As a result,a quadratic polynomial mathematical model was built.The optimal extraction conditions of RSM were determined as follows:Gynostemma pentaphyllum were suspended in microwave power of 400 W,subjected to ultrasonic treatment for 60 min at temperature of 51℃,80% ethanol concentration at solvent-to-solid ratio 28∶1(mL/g)and then microwaves 117 s.The resultofverification experiment(7.05%)was coincided with predictive value.
文章编号:201612012     中图分类号:    文献标志码:
基金项目:福建省教育厅科技项目(JA12218);福建省教育厅科技项目(JA15310)
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