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投稿时间:2015-01-19
投稿时间:2015-01-19
中文摘要: 以绞股蓝为原料,采用微波超声双辅助提取皂苷。在单因素试验的基础上,采用响应面分析法优化提取工艺,建立二次多项数学模型。结果表明,绞股蓝皂苷微波超声双辅助提取的最优工艺参数为:微波功率400 W、超声时间60 min、乙醇浓度80%、超声温度为51℃、微波时间117 s、液料比28∶1(mL/g),此条件下绞股蓝皂苷提取率为7.05%,与预测值的相对误差约为0.57%,试验值与预测值相吻合。
Abstract:The microwave-ultrasonic-assisted extraction ofsaponins from Gynostemma pentaphyllum was optimized using response surface methodology.Base on single-factor experiments,the extraction conditions ofmicrowave-ultrasonic-assisted extraction yield of saponins in the Gynostemma pentaphyllum were by RSM.As a result,a quadratic polynomial mathematical model was built.The optimal extraction conditions of RSM were determined as follows:Gynostemma pentaphyllum were suspended in microwave power of 400 W,subjected to ultrasonic treatment for 60 min at temperature of 51℃,80% ethanol concentration at solvent-to-solid ratio 28∶1(mL/g)and then microwaves 117 s.The resultofverification experiment(7.05%)was coincided with predictive value.
keywords: response surface methodology microwave-ultrasonic-assisted extraction Gynostemma pentaphyllum saponins
文章编号:201612012 中图分类号: 文献标志码:
基金项目:福建省教育厅科技项目(JA12218);福建省教育厅科技项目(JA15310)
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