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投稿时间：2015-06-13
投稿时间：2015-06-13
中文摘要: 利用单因素试验和正交试验的方法，研究在微波辅助下，以乙醇为萃取剂提取新疆南疆地区玫瑰花中总黄酮 的工艺条件， 并对提取的总黄酮进行定性分析与吸附纯化。结果表明，最佳提取工艺条件是乙醇浓度 50 %、料液比 1 ∶ 20（g/mL）、微波时间 40 s、微波功率 900 W、提取 2 次。此条件下玫瑰花中总黄酮含量为 3.73 %。通过颜色反应初步鉴 定玫瑰花黄酮提取液， 确定其中含有黄酮及黄酮醇类等成分。利用 AB-8 大孔树脂吸附纯化玫瑰花总黄酮，通过吸附、 解吸实验，结果显示，吸附率 37.58 %，解析率 48.50 %，纯度 25.4 %。
Abstract:Using single factor and orthogonal test method， studied on microwave -assisted extracting total flavonoids from rose in Southern Xinjiang ， and the extraction of flavonoids were qualitatively analyzed and adsorption purification. The results showed that the optimum extracting technology were as follows：alcohol contraction 50 %，solid-liquid ratio 1 ∶ 20 （g/mL）， microwave extraction time 40 s， microwave power 900 W， extraction 2 times. On these conditions， the total content of flavonoids in the roses was 3.73 %. Flavone and flavonol were identified by initial color authentication in flavonoids.The AB-8 macroporous resin was used to purify total flavonoids of rose， adsorption and desorption experiment results showed that： adsorption rate 37.58 %，desorption rate 48.50 %， purity 25.4 %.
文章编号：201603025 中图分类号： 文献标志码：A
基金项目:教育部“春晖计划”合作科研项目（Z2006-1-83001）
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