超临界CO2萃取竹叶花椒挥发油的工艺优化

李潮俊1; 2; 张玉1; 陈凯2; 康明1; 梁晓峰1; 2*

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DOI:10.12161/j.issn.1005-6521.2023.023.014

食品研究与开发:2023,44(23):99-104

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超临界CO2萃取竹叶花椒挥发油的工艺优化

李潮俊1，2，张玉1，陈凯2，康明1，梁晓峰1，2*^1,2

(1．西南科技大学材料与化学学院，四川绵阳 621010;2．四川中医药高等专科学校川西北中药材资源研究与开发利用实验室，绵阳市中药资源开发利用重点实验室，四川绵阳 621010)

Optimization of Supercritical CO2 Extraction Process of Volatile Oil from Zanthoxylum armatum DC.

LI Chaojun1，2，ZHANG Yu1，CHEN Kai2，KANG Ming1，LIANG Xiaofeng1，2*^1,2

(1.School of Materials and Chemistry，Southwest University of Science and Technology，Mianyang 621010，Sichuan，China;2.Laboratory of Research and Development and Utilization of Chinese Medicinal Materials in Northwest Sichuan，Mianyang Key Laboratory of Traditional Chinese Medicine Resources Development and Utilization，Sichuan College of Traditional Chinese Medicine，Mianyang 621010，Sichuan，China)

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投稿时间：2022-07-29

中文摘要: 该研究使用超临界CO2 萃取技术提取竹叶花椒挥发油，通过单因素试验，选择萃取时间、萃取温度、萃取压力为主要影响因素，采用Box-Behnken 响应面法，以竹叶花椒挥发油提取率为响应指标，建立超临界CO2萃取竹叶花椒挥发油的响应面模型，结合实际情况进行调整，获得最佳工艺条件。结果表明：在萃取时间80 min、萃取温度50.5 ℃、萃取压力25.5 MPa、分离釜Ⅰ压力6 MPa、温度45 ℃的条件下挥发油提取率为14.25%，与预测结果相符。

中文关键词: 竹叶花椒挥发油超临界萃取提取工艺提取率

Abstract:The supercritical CO2 extraction technology was used to extract the volatile oil of Zanthoxylum armatum DC..The extraction time，temperature，and pressure were selected as the main influencing factors by the single factor tests and optimized by the Box-Behnken design-response surface method with the extraction rate of the volatile oil as the indicator.The optimal extraction conditions were determined considering the actual conditions.The results showed that the extraction rate of volatile oil was 14.25% when the extraction was carried out at extraction temperature of 50.5 ℃the extraction pressure of 25.5 MPa，the separation I pressure of 6 MPa，and temperature of 45 ℃for 80 min，which was consistent with the predicted results.

keywords: Zanthoxylum armatum DC. volatile oil supercritical extraction extraction process extraction rate

文章编号：202323014 中图分类号： 文献标志码：

基金项目:四川省中医药管理局科学技术研究专项课题（2020JC0120）；绵阳市科技项目（2020YFZJ004）；四川省中医药重点学科中药化学学科建设项目（川中医药函〔2020〕84 号）

作者	单位
李潮俊1，2，张玉1，陈凯2，康明1，梁晓峰1，2*	1．西南科技大学材料与化学学院，四川绵阳 621010；2．四川中医药高等专科学校川西北中药材资源研究与开发利用实验室，绵阳市中药资源开发利用重点实验室，四川绵阳 621010

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Affiliation

LI Chaojun1，2，ZHANG Yu1，CHEN Kai2，KANG Ming1，LIANG Xiaofeng1，2*

1.School of Materials and Chemistry，Southwest University of Science and Technology，Mianyang 621010，Sichuan，China；2.Laboratory of Research and Development and Utilization of Chinese Medicinal Materials in Northwest Sichuan，Mianyang Key Laboratory of Traditional Chinese Medicine Resources Development and Utilization，Sichuan College of Traditional Chinese Medicine，Mianyang 621010，Sichuan，China

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