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食品研究与开发:2022,43(12):114-123
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响应面法优化DHA藻油微胶囊工艺
(1.齐鲁工业大学(山东省科学院)食品科学与工程学院,山东 济南 250353;2.山东中硕海洋科技有限公司,山东 日照 276800)
Optimization of DHA Algal Oil Microcapsule Processing Using Response Surface Methodology
(1.School of Food Science and Engineering,Qilu University of Technology(Shandong Academy of Sciences),Jinan 250353,Shandong,China;2.Shandong Zhongshuo Marine Technology Co.,Ltd.,Rizhao 276800,Shandong,China)
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投稿时间:2021-05-20    
中文摘要: 以阿拉伯胶、β-环糊精作为复合壁材,二十二碳六烯酸(docosahexaenoic acid,DHA)藻油为芯材,通过喷雾干燥法制备DHA藻油微胶囊。采用单因素试验结合响应面试验优化DHA藻油微胶囊制备工艺,得到最佳制备条件:壁材质量比(β-环糊精∶阿拉伯胶)1∶2.82,芯壁质量比 1∶2.3,固形物浓度 16%,进料速度 15.5 r/min,进风温度 167℃,包埋率为94.87%。通过傅里叶红外光谱仪、扫描电镜、激光粒度仪、热重分析仪对微胶囊结构、形态进行表征。结果表明微胶囊结构完整,外壁未出现破损、孔洞,包埋效果较好,粒径分布集中,并且具有良好的热稳定性,符合大多数食品加工温度的要求。
中文关键词: DHA藻油  微胶囊  响应面  工艺优化  喷雾干燥
Abstract:Using gum arabic and β -cyclodextrin as the composite wall material and docosahexaenoic acid(DHA)algal oil as the core material,microcapsules were prepared by spray drying.A single factor experiment combined with a response surface methodology experiment optimized the preparation process.The optimum preparation conditions employed were as follows:wall material mass ratio(β-cyclodextrin:acacia),1∶2.82;core wall mass ratio,1∶2.3;solids concentration,16%;feed rate,15.5 r/min;inlet air temperature,167 ℃;microencapsulation efficiency,94.87%.The structure and morphology of microcapsules were characterized by Fouriertransform infrared spectrometry,scanning electron microscopy,laser particle size analysis,and thermogravimetric analysis.The results revealed a complete microcapsule structure,with no damage or holes on the outer wall,good embedding effect,concentrated particle size distribution,and good thermal stability.These attributes meet the requirements of most food processing temperatures.
文章编号:202212016     中图分类号:    文献标志码:
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