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食品研究与开发:2022,43(7):167-174
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基于电子鼻及气相-离子迁移谱法分析阳光玫瑰葡萄贮藏期挥发性成分
(1.广西壮族自治区农业科学院葡萄与葡萄酒研究所,广西 南宁 530007;2.广西壮族自治区农业科学院农产品质量安全与检测技术研究所,广西 南宁 530007)
Analysis of Volatile Components of Shine Muscat Grapes during Storage Periods by Electronic Nose and GC-IMS
(1.Grape and Wine Research Institute,Guangxi Academy of Agricultural Sciences,Nanning 530007,Guangxi,China;2.Agro-Products Quality Safety and Testing Technology Research Institute,Guangxi Academy of Agricultural Sciences,Nanning 530007,Guangxi,China)
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投稿时间:2021-05-13    
中文摘要: 为探索阳光玫瑰葡萄贮藏期香气变化规律,采用电子鼻及气相-离子迁移谱法(gas chromatography-ion mobility spectrometry,GC-IMS)分析2个贮藏温度下阳光玫瑰葡萄贮藏期挥发性成分变化规律。结果表明:GC-IMS共鉴定出33种成分,贮藏6周内特征风味物质为里那醇、(E)-2-戊烯醛等,表现玫瑰香和果香;贮藏8周至12周乙酸乙酯含量增加,表现出果香、酯香和酒香,存在香气品质劣变;16周至20周,己醇、乙醇等含量增加,典型香气发生变化;温度因素对贮藏期特征风味物质变化趋势作用明显,0℃下特征风味物质逸损明显;主成分分析(principal component analysis,PCA)结果表明,0℃处理的样品分离度更明显,10℃处理在部分贮藏期更接近,变化相对小。电子鼻能较好区分不同贮藏期样品,香气差异主要集中于萜烯敏感的W1W传感器。
Abstract:This study aimed to explore the changes in aroma of the Shine Muscat grape during storage.The electronic nose and gas chromatography-ion mobility spectrometry(GC-IMS)were used to detect the volatile components of Shine Muscat grapes during storage at two different temperatures.A total of 33 compounds were identified by GC-IMS.The characteristic flavor compounds of the stored grape samples throughout the first 6 weeks included linalool and(E)-2-pentenal,which were associated with rose and fruit fragrances.The characteristic compound of the stored grape samples from 8 to 12 weeks was ethyl acetate,which had a fruity,ester,and wine aroma.This indicated a certain degree of deterioration.From 16 to 20 weeks,1-hexanol,ethanol,and other characteristic compounds caused an obvious change in the typical aroma characteristics.There were significant differences in the variation trends of characteristic flavor compounds at different temperatures during the storage period,and the loss of characteristic flavor compounds was greater at 0℃.The principal component analysis(PCA)results showed that the samples stored at 0℃ could be better separated,the samples stored at 10℃ became more closer at some storage periods,indicated minor changes.Samples collected after different storage periods could be distinguished well using the electronic nose.The differences between the samples were mainly concentrated on the W1W sensor.Key words:Shine Muscat grape;volatile components;storage period;electronic nose;gas chromatography-ion mobility spectrometry(GC-IMS)
文章编号:202207024     中图分类号:    文献标志码:
基金项目:广西重点研发计划(桂科AB18221077);广西农业科学院科技发展基金(桂农科2021JM107);广西农业科学院基本科研业务专项(桂农科2020YM51)
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