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食品研究与开发:2021,42(24):155-160
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利用同相等差感应电势法检测膨化食品中阿斯巴甜的研究
(1.广东利诚检测技术有限公司,广东 中山 528436;2.华南农业大学食品学院,广东 广州 510642;3.江南大学食品学院,江苏 无锡 214122;4.英都斯特(无锡)感应科技有限公司,江苏 无锡 214035)
Determination of Aspartame in Puffed Food Using In-phase Equal-Difference Induction Potential Method
(1.Guangdong Licheng Detection Technology Co.,Ltd.,Zhongshan 528436,Guangdong,China;2.College of Food Science,South China Agricultural University,Guangzhou 510642,Guangdong,China;3.School of Food Science and Technology,Jiangnan University,Wuxi 214122,Jiangsu,China;4.INDUC Scientific Co.,Ltd.,Wuxi 214035,Jiangsu,China)
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投稿时间:2021-07-23    
中文摘要: 利用同相等差感应电势法,向初级线圈施加5 V~20 V激励电压和300 Hz~500 Hz频率的激励参数,探究次级线圈中阿斯巴甜溶液的电学特性。结果发现,0~100 mg/kg阿斯巴甜溶液的瞬时绝对电压与初级线圈激励电压大小呈正相关,但不随频率变化而改变。20 V、300 Hz条件下,100 mg/kg阿斯巴甜溶液电势差较50 mg/kg提高32.46%,当阿斯巴甜质量分数增加时,体系电势差随激励电压增加而增大。阿斯巴甜质量分数、激励电压、频率及体系电势差呈线性相关,相关系数(r)为0.94。利用同相等差感应电势与化学法检测5种市售膨化食品中的阿斯巴甜总含量,其检测结果相对误差均在2.50%以内,同相等差感应电势法具有良好的重复性和准确性。将膨化食品预处理后的料液作为次级线圈,通过同相等差感应电势法测定其电信号特性来量化阿斯巴甜总含量,为膨化食品中阿斯巴甜的检测提供了一种新技术方法。
Abstract:In this study,5 V-20 V excitation voltage and 300 Hz-500 Hz excitation frequency were applied to a primary coil using the in-phase equal-difference induction potential method to analyze the electrical characteristics of aspartame solution in the secondary coil.The results showed that the instantaneous absolute voltage of 0-100 mg/kg aspartame solution positively correlated with the excitation voltage of the primary coil but did not change with the frequency.At 20 V and 300 Hz,the potential difference of 100 mg/kg aspartame solution was 32.46% higher than that of 50 mg/kg.When the mass fraction of aspartame increased,the potential difference of the system increased with increasing excitation voltage.The correlation coefficient(r)was 0.94,and the relative error was less than 2.50%.The method showed good repeatability and accuracy.The pretreated liquid of puffed food was used as the secondary coil,and its electrical signal characteristics were determined using the in-phase equal-difference induction potential method to quantify the total aspartame content.The proposed method is valuable for detecting aspartame in puffed food.
文章编号:202124023     中图分类号:    文献标志码:
基金项目:中国博士后科学基金项目(2020M682725);国家自然科学基金面上项目(32172353);江苏省优秀青年基金项目(BK20211582)
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