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食品研究与开发:2021,42(23):137-144
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不同冷冻复温条件下南果梨可溶性固形物含量的高光谱表征方法研究
(天津商业大学 天津市制冷技术重点实验室,天津 300134)
Hyperspectral Characterization of Soluble Solids in Nanguo Pear under Different Freezing-Thawing Conditions
(Tianjin Key Lab of Refrigeration Technology,Tianjin University of Commerce,Tianjin 300134,China)
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投稿时间:2021-05-18    
中文摘要: 采用高光谱方法表征在不同冷冻复温条件下南果梨可溶性固形物含量变化的特征,设置不同的冷冻复温条件(临界温度、循环次数、保温时间以及降温速率),采集其高光谱反射的光谱图像,并进行可溶性固形物含量测定。采用4种不同的预处理方式[多元散射校正(multiplicative scatter correction,MSC)、标准正态变量交换(standard normal variate,SNV)、平滑-标准正态变量交换(Savitzky-Golay standard normal variate,S-G-SNV)、平滑-多元散射校正(Savitzky-Golay multiplicative scatter correction,S-G-MSC)]并结合竞争性自适应重加权算法(competitive adaptive reweighted sampling,CARS)所识别的特征光谱,通过偏最小二乘法(partial least squares method,PLS)建立南果梨不同冷冻-复温条件下获得的可溶性固形物模型。结果表明:高光谱能够良好反映南果梨可溶性固形物的含量变化。在不同循环次数下,S-G-MSC-CARS-PLS模型精度最高;在不同降温速率下,MSC-CARS-PLS模型精度最高;在不同保温时间下,SNV-CARS-PLS模型精度最高;在不同临界温度下,S-G-SNV-CARS-PLS模型精度最高。
Abstract:The hyperspectral method was used to characterize various soluble solid contents of Nanguo pear under different freezing and rewarming conditions such as critical temperature,cycle time,holding time,and cooling rate.Hyperspectral reflection images were collected and the soluble solid contents were determined.Using four different pretreatment methods[multiplicative scatter correction (MSC),standard normal variate(SNV),Savitzky-Golay standard normal variate(S-G-SNV),and Savitzky-Golay multiplicative scatter correction (S-G-MSC)]and the characteristic spectra identified by competitive adaptive reweighted sampling(CARS),the soluble solid model of Nanguo pear under different freezing and rewarming conditions was established by partial least squares method(PLS).The results showed that the hyperspectra reflect the changes in the soluble solid contents of Nanguo pear.The accuracy of S-G-MSC-CARS-PLS model was the highest under different cycles of freezing treatment.Under different cooling rates,the accuracy of MSC-CARS-PLS model was the highest.The accuracy of SNV-CARS-PLS model was the highest at different holding time.The accuracy of S-G-SNV-CARS-PLS model was the highest at different critical temperatures.
文章编号:202123022     中图分类号:    文献标志码:
基金项目:国家自然科学基金项目(12172254、11772225);天津市自然科学基金项目(18JCQNJC77300、19JCTPJC52900);天津市研究生科研创新项目(2020YJSS066)
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