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投稿时间：2019-01-11
投稿时间：2019-01-11
中文摘要: 建立固相萃取-气相色谱-三重四极杆质谱测定方便面中16 种多环芳烃的方法。方便面样品用正己烷和乙腈-丙酮提取，经Oasis HLB 和Florisil 柱两步净化，气相色谱-三重四极杆质谱检测。在试验浓度范围内，线性关系良好，各种多环芳烃的定量限在0.03 μg/kg～0.54 μg/kg 之间。在不同的加标浓度下，加标回收率在75%～129%之间，相对标准偏差小于13.4%。该方法快速、准确、灵敏度高、重现性好，适用于大批量样品中多环芳烃的快速测定。
Abstract:The method for analysis of polycyclic aromatic hydrocarbons in instant noodles was established by solid phase extraction coupled with gas chromatography -triple quadrupole mass spectrometry（GC-MS/MS）.The samples of instant noodles were extracted by n-hexane and acetonitrile-acetone.Extract was purified by Oasis HLB and Florisil solid phase column and detected by GC-MS/MS.The linear relationship was good within the experimental concentration range，and the limit of quantification of various polycyclic aromatic hydrocarbons was between 0.03 μg/kg and 0.54 μg/kg.Under different spiked concentrations，the recoveries ranged from 75 % to 129 % with a relative standard deviation of less than 13.4 %.The method was fast，accurate，sensitive and reproducible，and suitable for rapid determination of polycyclic aromatic hydrocarbons in large samples.
keywords: polycyclic aromatic hydrocarbons instant noodle gas chromatography-triple quadrupole mass spectrometry solid phase extraction purification
文章编号：202001027 中图分类号： 文献标志码：
基金项目:淄博市科技发展计划项目（2017kj010071）；山东省医药卫生科技发展计划项目（2017WS378）
| 作者 | 单位 |
| 邢燕，王敏，刘玉栋，王勤，赵军溪 | 淄博市疾病预防控制中心，山东淄博255026；淄博市环境有机污染与人群健康监测分析重点试验室，山东淄博255026；淄博市科学技术情报研究所，山东淄博255025 |
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