Abstract:Under the optimum conditions of pretreatment and instrument parameters，the gas chromatographymass spectrometry was applied on a comprehensive qualitative and quantitative analytical method of fifteen terpenols ester compounds in food flavors.The internal standard method had been applied for quantitative analysis，the chromatographic peaks of the target compounds and internal standard had achieved the high resolution，presented a good linear relationship in the concentration range of 2 μg/mL-40 μg/mL，and the detection limits were 1.95 mg/kg-4.01 mg/kg.The average spiked recoveries were in the range from 83.4%to 113.8%，and the relative standard deviations were all less than 5.0%.