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投稿时间：2016-11-24
投稿时间：2016-11-24
中文摘要: 建立高效液相色谱-串联质谱法（LC-MS/MS）测定小杂粮中氨基甲酸酯类农药残留分析方法。样品以乙腈为 提取剂，超声波提取。该方法加标回收率平均值为 83.5 %~103 %，检出限在 0.006 μg/kg~0.031 μg/kg，定量限在
0.016 μg/kg~0.085 μg/kg 范围内，相对标准偏差在 0.83 %~5.8 %范围内。
中文关键词: 高效液相色谱-串联质谱 小杂粮 农药残留
Abstract:A high-performance liquid chromatography-tandem mass spectrometry was developed for the deter－ mination of carbamate pesticide residues of minor food crops. The samples were extracted by ultrasonic extrac－ tion with acetonitrile， the average spiked recovery of this method was range from 83.5 % to 103 %. Limit of de－ tection were in 0.006 μg/kg-0.031 μg/kg， limit of quantitation were in 0.016 μg/kg-0.085 μg/kg. Relative stan－ dard deviation were in 0.83 %-5.8 %.
keywords: high-performance liquid chromatography-tandem mass spectrometry minor food crops pesticide residues
文章编号：201705037 中图分类号： 文献标志码：A
基金项目:忻州师范学院院级青年基金项目（No.QN201401）
| Author Name | Affiliation |
| ZHANG Ting， ZHAO Er-lao， REN Guang-ming， FAN Jian-feng | Department of Chemistry， Xinzhou Teachers University， Xinzhou 034000， Shanxi， China |
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